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描述
Oxygen Analyzer
1.Public environmental condition
| Number | 物品 | Environmental conditions | 笔记 |
| 1 | service voltage | 220电压±10%,50±2%Hz | |
| 2 | ground resistance | <5哦(Separate ground cable required) | |
| 3 | 湿度 | <80%相对湿度,An air conditioner is required to be installed in the operation room | |
| 4 | 环境温度 | 18℃~29℃ | |
| 5 | electromagnetic interference, vibration | No high frequency electromagnetic field, no strong vibration source | |
| 6 | carrier gas | 氩气, 纯度 99.999% | |
| 7 | power gas
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氮, industrial pure |
2.Design, manufacture, installation and acceptance of legal standards and standards
| Number | Legal specification standard name
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笔记 |
| 1 | 国标/T 11261-2006 Determination of oxygen content of iron and steel – pulse heating inert gas melting – infrared absorption method
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3.Equipment and supporting materials purchase list
| Number | 姓名 | Factory owner
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数量
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笔记 |
| 1 | Oxygen analyzer main engine
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1 piece | 标准配置 | |
| 2 | Standard spare parts are provided
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For details, see the spare parts list | 1 放 | 标准配置 |
| 3 | analysis software | 1 放 | 标准配置 | |
| 4 | Instrument instruction manual | a copy | 标准配置 | |
| 5 | Cooling circulation system | 2 HP cooling capacity | 1 放 | 标准配置 |
| 6 | 打印机 | HP printer | 1 piece | 标准配置 |
| 7 | electronic scales | Sartorius 1/10,000 准确性 | 1 piece | 标准配置 |
| 8 | 电脑 | Industrial Personal Computer | 1 放 | 标准配置 |
| 9 | voltage-stabilized source | 10千伏安 | 1 piece | 标准配置 |
| 10 | standard sample | One set according to customer needs | 1 放 | 标准配置 |
4.时间echnical requirements
1、Major parts requirements
| Number | 姓名 | Brand or technical requirements | 笔记 |
| 1 | 检测系统 | German brand | 标准配置 |
| 2 | pneumatic element | Italian brand | 标准配置 |
| 3 |
Pulse furnace
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water-cooled transformer | 标准配置 |
| 4 | linear power supply | Aerospace Science and Industry Group Chaoyang Changfeng | 标准配置 |
| 5 | temperature control system | Taiwan brand | 标准配置 |
| 6 | power controller | Taiwan brand | 标准配置 |
2、Equipment technical specifications requirements
| Number | 物品 | require | 笔记 |
| 1 | Principle and application | The oxygen in metal and non-metal solid materials is detected by inert gas melting principle. In the determination of oxygen, the sample after weighing is placed in a graphite crucible and melted by heating at high temperature in the argon gas flow. The oxygen in the sample reacts with the carbon in the graphite crucible to produce carbon monoxide (一氧化碳). This mixture is sent by argon gas to the reformer, where the carbon monoxide (一氧化碳) is converted to carbon dioxide (二氧化碳), and through the gas mixture after the reformer is sent to the infrared detection tank, where carbon dioxide (二氧化碳) is detected. Rapid and accurate determination of oxygen content in steel, cast iron, alloys, 铜, zirconium, 钛, rare earth materials, nanomaterials and other inorganic substances.
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| 2 | analytical range | Oxygen: 0.00001% 〜 20%(expandable measurement range)
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| 3 | analytical precision | Oxygen: 1ppm or RSD≤1%
笔记: not greater than the sample standard deviation or uncertainty shall prevail.
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| 4 | 灵敏度 | 0.01百万分之一 | |
| 5 | parsing time | Usually 3 分钟
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| 6 | 检测系统 | Non-dispersive infrared detection system was used for oxygen analysis
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| 7 | Infrared detection system | 1, the standard configuration oxygen analyzer is equipped with an independent infrared absorption pool, and the length and number of channels can be flexibly configured according to user needs;
2, 发动机: the modulation system adopts single-chip microcomputer control of high-precision stepper motor, to achieve long-term stability of the modulation frequency;
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| 8 | Sample weighing | 0.01-1G,Sample size can be changed according to sample content
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| 9 | Pulse furnace
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1, 当前的 0 ~ 1500A, 力量: 10千伏安, the highest temperature is higher than 3200℃.
2, pulse electrode furnace heating temperature is high, using program control power, can provide constant power heating, slope heating, segmented heating and other program heating methods, improve the analysis accuracy. It is suitable for rapid analysis from low melting point materials such as aluminum alloy to high melting point materials such as tungsten alloy. The electrode is suitable for a variety of types of crucible, according to the release of different samples, can choose a variety of crucible including sleeve crucible, high temperature crucible, effectively reduce the user’s use cost. The electrode cooling system adopts a single cycle independent cooling system, which can directly connect the circulating water or the external water cooling device, and has the characteristics of good cooling effect and high reliability.
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| 10 | gas circuit | 1, the use of integrated whole machine design, open space, the gas path system connection route is greatly reduced, the whole gas path system is more concise and reliable. Gas components including solenoid valve, cylinder, gas pipe, gas joint all adopt imported components, solenoid valve life of more than one million times. The special lifting system with two-axis guide cylinder ensures the smooth lifting of the electrode, ensures the good contact between the graphite crucible and the upper electrode, and ensures the uniform force of the graphite crucible, which is conducive to long-term high temperature heating. Automatic blanking furnace head with air curtain protection and automatic air purging mechanism effectively ensure the accuracy of oxygen element analysis. The furnace head is a split structure, easy to disassemble and replace, and the lower electrode is made of high-temperature alloy material, long service life and low cost. (If the whole furnace head is used, the replacement of the electrode requires professional and technical personnel to operate, which is very troublesome).
2, the design of the sampling system is open, its advantage is that the pollutants are discharged from the top of the furnace, not into the system, 易于操作, the system sealing requirements are not high.(Closed, the gas path through a costly six-way valve to control, internal out.(Some companies have complex sampling device, there are two cylinders, such as the sample stuck, need to open the cylinder, difficult to take out). The micro-flow sensor is used to achieve high precision flow control, and the influence of analysis air flow changes on the analysis is minimized. Gas conversion through this valve, so that the valve is easy to break, dust and other pollutants are also easy to bring into the system). This injection device is simple and can be automatically injected, in case the sample is stuck, easy to remove
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| 11 | Power gas
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Nitrogen or water-free oil-free compressed air
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| 12 | revise | 1. Single point correction: correction with a single analysis result
2, multi-point correction: with multiple analysis results correction
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| 13 | 电源 | 1, pulse furnace power supply: 220VAC 10%, 501赫兹, maximum current 50A.
2. Other power supply of the instrument: 220VAC 10%, 501赫兹, maximum current 10A.
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| 14 | software function | 1. Provide software under Windows environment to quickly display analysis results and analysis curves;
2. Automatic storage of analysis results;
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| 15 | routine test |
Instrument inspection and calibration certificate
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5.Provide equipment data requirements
| Number | 姓名 | 笔记 |
| 1 | manufacturer certificate | |
| 2 | Operating standards for equipment operation, inspection and maintenance | |
| 3 | Spare parts list of the whole set | |
| 4 | Machine operation manual. | |
| 5 | Operating instructions for main parts. |
6.Spare parts list
| 6A-101 | Graphite external crucible | 100 Pieces | ||
| 6A-102 | Graphite internal crucible | 300 Pieces | ||
| 6A-103 | decompressing table | 2 Pieces | ||
| 6A-104 | hairbrush | 1 Piece | ||
| 6A-105 | instruction book | 1 Piece | ||
| 6A-106 | cleanroom wiper | 1 Piece | ||
| 6A-107 | High temperature electrode sheet | 1 Piece | ||
| 6A-108 | Seal spare parts | 1 Set | ||
| 6A-109 | Sample tweezers | 1 Piece | ||
| 6A-110 | Crucible tweezers | 1 Piece | ||
| 6A-111 | Pagoda copper brush | 1 Piece | ||
| 6A-112 | Injector cleaning brush | 1 Piece | ||
| 6A-113 | air pipe line Φ6 | 20 Meters | ||
| 6A-114 | Vacuum silicone grease | 1 Piece | ||
| 6A-115 | High efficiency dehydrating agent | 1 Piece | ||
| 6A-116 | CO2absorbent | 1 Piece | ||
| 6A-117 | quartz wool | 1 Piece | ||
| 6A-118 | water pipe | 20 Meters | ||
| 6A-119 | Rare earth copper oxide | 1 Piece | ||
| 6A-120 | High temperature quartz tube | 1 Piece | ||
| 6A-121 | Reagent quartz tube | 1 Piece | ||
| 6A-122 | Filtered quartz tube | 1 Piece | ||
| 6A-123 | certificate | 1 Piece | ||
| 6A-124 | Nickel basket | 1 Piece | ||
| 6A-125 | Nickel pocket | 1 Piece | ||
| 6A-126 | Electrode cleaning copper brush | 1 Piece |










